tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

Base Information

Chemical Name:tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane
CAS No.:868593-28-6
Molecular Formula:C₁₆H₃₂O₄Si
Molecular Weight:316.513
Hs Code.:

Synonyms:tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

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Chemical Property of tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

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Technology Process of tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

There total 9 articles about tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 868593-26-4
(3aR,4R,5R,7R,7aR)-4-(tert-Butyl-dimethyl-silanyloxy)-7-methoxymethoxy-5-methoxymethyl-hexahydro-benzo[1,3]dioxole-2-thione

: 868593-28-6
tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

Guidance literature:: With 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine;
DOI:10.1055/s-2005-872222

Reference yield:

: 868593-19-5
C₁₅H₂₄O₅

: 868593-28-6
tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 6 steps

1.1: 87 percent / NaH / tetrahydrofuran; dimethylformamide

2.1: BH₃*SMe₂ / -20 °C

2.2: 92 percent / NaBO₃*4H₂O / tetrahydrofuran

3.1: 90 percent / imidazole / dimethylformamide

4.1: 90 percent / TsOH / methanol / 20 °C

5.1: 82 percent / toluene / 5 h / Heating

6.1: 90 percent / 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidene

With 1H-imidazole; 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine; dimethylsulfide borane complex; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-2005-872222

Reference yield:

: 868593-20-8
C₁₆H₂₆O₅

: 868593-28-6
tert-Butyl-((1S,4R,6R)-4-methoxymethoxy-6-methoxymethyl-cyclohex-2-enyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 5 steps

1.1: BH₃*SMe₂ / -20 °C

1.2: 92 percent / NaBO₃*4H₂O / tetrahydrofuran

2.1: 90 percent / imidazole / dimethylformamide

3.1: 90 percent / TsOH / methanol / 20 °C

4.1: 82 percent / toluene / 5 h / Heating

5.1: 90 percent / 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidene

With 1H-imidazole; 1,3-dimethyl-2-phenyl-1,3,2-diazaphospholidine; dimethylsulfide borane complex; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-2005-872222