N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

Base Information

Chemical Name:N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine
CAS No.:145487-44-1
Molecular Formula:C₅₂H₇₀N₄O₁₀
Molecular Weight:911.149
Hs Code.:

Synonyms:N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

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Technology Process of N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

There total 2 articles about N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.2%

: 124-09-4
1,6-Hexanediamine

: 145487-43-0
ethyl 3-(tetrahydropapaverin-2'-yl)propionate

: 145487-44-1
N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; for 24h; Ambient temperature;
DOI:10.1016/0223-5234(92)90180-9

Reference yield:

: 13074-31-2
Tetrahydropapaverine

: 145487-44-1
N,N'-4,11-diaza-3,12-dioxotetradecylene-1,14-diyl-bis-(R,S)-tetrahydropapaverine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / glacial acetic acid / 4 h / 70 °C

2: 71.2 percent / NaH / dimethylsulfoxide / 24 h / Ambient temperature

With sodium hydride; acetic acid; In dimethyl sulfoxide;
DOI:10.1016/0223-5234(92)90180-9