4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

Base Information

Chemical Name:4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde
CAS No.:936133-25-4
Molecular Formula:C₂₆H₃₇NO₃
Molecular Weight:411.585
Hs Code.:

Synonyms:4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

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Chemical Property of 4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

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Technology Process of 4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

There total 4 articles about 4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 936133-19-6
4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzonitrile

: 936133-25-4
4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2007.02.053

Reference yield:

: 24596-19-8
4-bromo-2,6-dimethylphenylamine

: 936133-25-4
4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / CuI; KI; N,N'-dimethylethylenediamine / dimethylformamide / 24 h / 100 °C

2: 76 percent / 2-(di-cyclohexylphosphino)biphenyl; t-BuONa / Pd₂(dba)3 / toluene / 19 h / 100 °C

3: 25 percent / NaH / dimethylformamide / 0 - 20 °C

4: 92 percent / diisobutylaluminium hydride / toluene / 0 - 20 °C

With copper(l) iodide; sodium hydride; diisobutylaluminium hydride; potassium iodide; sodium t-butanolate; N,N`-dimethylethylenediamine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2007.02.053

Reference yield:

: 74896-24-5
4-amino-3,5-dimethylbenzonitrile

: 936133-25-4
4-[N-(n-hexyl)-N-[3-isopropyl-4-(methoxymethoxy)phenyl]amino]-3,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 2-(di-cyclohexylphosphino)biphenyl; t-BuONa / Pd₂(dba)3 / toluene / 19 h / 100 °C

2: 25 percent / NaH / dimethylformamide / 0 - 20 °C

3: 92 percent / diisobutylaluminium hydride / toluene / 0 - 20 °C

With sodium hydride; diisobutylaluminium hydride; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2007.02.053