Technology Process of Tetrabenzyl N4-tosyl-1,2,4-butanetriamine-N1,N1,N2,N2-tetraacetate
There total 4 articles about Tetrabenzyl N4-tosyl-1,2,4-butanetriamine-N1,N1,N2,N2-tetraacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium iodide;
In
acetonitrile;
for 44h;
Heating;
DOI:10.1055/s-1989-27402
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) 10percent aq. KOAc, 2.) MeOH / 1.) CH3CN, r.t., 70 h, 2.) 70 deg C, 2 h
2: 19 percent / H2 / 10percent Pd/C / methanol / 94 h / 50 °C / 4200.3 Torr
3: 95 percent / 18percent aq. HCl / methanol / 3 h / Ambient temperature
4: 20 percent / N,N,N',N'-tetramethyl-1,8-naphthalenediamine, NaI / acetonitrile / 44 h / Heating
With
hydrogenchloride; methanol; hydrogen; potassium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium iodide;
palladium on activated charcoal;
In
methanol; acetonitrile;
DOI:10.1055/s-1989-27402
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 19 percent / H2 / 10percent Pd/C / methanol / 94 h / 50 °C / 4200.3 Torr
2: 95 percent / 18percent aq. HCl / methanol / 3 h / Ambient temperature
3: 20 percent / N,N,N',N'-tetramethyl-1,8-naphthalenediamine, NaI / acetonitrile / 44 h / Heating
With
hydrogenchloride; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium iodide;
palladium on activated charcoal;
In
methanol; acetonitrile;
DOI:10.1055/s-1989-27402
