N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

Base Information

Chemical Name:N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide
CAS No.:126423-61-8
Molecular Formula:C₁₆H₁₉NO₄S
Molecular Weight:321.397
Hs Code.:

Synonyms:N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

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Chemical Property of N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

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Technology Process of N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

There total 6 articles about N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99440-81-0
endo-4-hydroxy-2-oxabicyclo<3.3.1>non-6-en-3-one

: 126423-61-8
N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / CrO₃, pyridine / CH₂Cl₂ / Ambient temperature

2: BF₃*Et₂O / 1,2-dichloro-ethane / 42 °C

3: NaCNBH₃ / 2-methyl-butan-2-ol / Ambient temperature

With pyridine; chromium(VI) oxide; boron trifluoride diethyl etherate; sodium cyanoborohydride; In tert-Amyl alcohol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja00311a110

Reference yield:

: 99440-80-9
Oxo-acetic acid cyclohex-3-enyl ester

: 126423-61-8
N-((1S,4R,5S)-3-Oxo-2-oxa-bicyclo[3.3.1]non-6-en-4-yl)-C-p-tolyl-methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / SnCl₄ / nitromethane / Ambient temperature

2: 86 percent / CrO₃, pyridine / CH₂Cl₂ / Ambient temperature

3: BF₃*Et₂O / 1,2-dichloro-ethane / 42 °C

4: NaCNBH₃ / 2-methyl-butan-2-ol / Ambient temperature

With pyridine; chromium(VI) oxide; boron trifluoride diethyl etherate; tin(IV) chloride; sodium cyanoborohydride; In tert-Amyl alcohol; nitromethane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja00311a110