benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside
CAS No.:83055-28-1
Molecular Formula:C₁₉H₂₇NO₇
Molecular Weight:381.426
Hs Code.:

benzyl 2-acetamido-2,6-dideoxy-3-O-<D-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

Synonyms:benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

There total 4 articles about benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 83114-31-2
benzyl 2-acetamido-4-O-acetyl-2,6-dideoxy-3-O--α-D-glucopyranoside

: 83055-28-1
benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

Guidance literature:: With methanol; Amberlite IR-120 (H⁺) resin; sodium methylate; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)80688-6

Reference yield:

: 40269-09-8
benzyl 2-acetamido-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

: 83055-28-1
benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / NBS, P(Ph)3 / dimethylformamide / 2 h / 50 °C

2: 99 percent / pyridine / Ambient temperature

3: 93 percent / azobis(isobutyronitrile), tributyltin hydride / toluene / 2 h / 100 - 110 °C

4: NaOMe / methanol / 1 h / 0 °C

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; triphenylphosphine; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1080/00021369.1980.10864112

Reference yield:

: Benzyl 2-acetamido-6-bromo-2,6-dideoxy-3-O--α-D-glucopyranoside

: 83055-28-1
benzyl 2-acetamido-2,6-dideoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / Ambient temperature

2: 93 percent / azobis(isobutyronitrile), tributyltin hydride / toluene / 2 h / 100 - 110 °C

3: NaOMe / methanol / 1 h / 0 °C

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; In methanol; toluene;
DOI:10.1080/00021369.1980.10864112