5-Bromo-2-iodobenzoyl chloride

Base Information

Chemical Name:5-Bromo-2-iodobenzoyl chloride
CAS No.:293738-03-1
Molecular Formula:C₇H₃BrClIO
Molecular Weight:345.362
Hs Code.:
European Community (EC) Number:657-355-5

Synonyms:5-bromo-2-iodobenzoyl chloride;293738-03-1;5-bromo-2-iodo-benzoyl chloride;YSZC277;5-bromo-2-iodobenzoylchloride;SCHEMBL5426640;Benzoyl chloride, 5-bromo-2-iodo-;AC5820;MFCD02063081;AKOS024275506;BS-52659;SY247915

Suppliers and Price of 5-Bromo-2-iodobenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-BROMO-2-IODO-BENZOYL CHLORIDE 95.00%
1G
$ 2436.00

American Custom Chemicals Corporation
5-BROMO-2-IODO-BENZOYL CHLORIDE 95.00%
5MG
$ 502.73

Alichem
5-Bromo-2-iodobenzoylchloride
250mg
$ 480.00

Alichem
5-Bromo-2-iodobenzoylchloride
1g
$ 1445.30

Alichem
5-Bromo-2-iodobenzoylchloride
500mg
$ 823.15

AK Scientific
5-Bromo-2-iodobenzoylchloride
5g
$ 728.00

Total 4 raw suppliers

Chemical Property of 5-Bromo-2-iodobenzoyl chloride

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:343.81005
Heavy Atom Count:11
Complexity:165

Purity/Quality:

97% ^*data from raw suppliers

5-BROMO-2-IODO-BENZOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1Br)C(=O)Cl)I

Technology Process of 5-Bromo-2-iodobenzoyl chloride

There total 3 articles about 5-Bromo-2-iodobenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21740-00-1
5-bromo-2-iodo-benzoic acid

: 293738-03-1
5-bromo-2-iodobenzoyl chloride

Guidance literature:: With thionyl chloride; for 1h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.05.040

Reference yield:

: 5794-88-7
5-Bromo-2-aminobenzoic acid

: 293738-03-1
5-bromo-2-iodobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium hydroxide; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere

1.2: 1.75 h / 40 - 90 °C / Inert atmosphere

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide; sodium nitrite; In dichloromethane; water;
DOI:10.1002/anie.201106786

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 293738-03-1
5-bromo-2-iodobenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine / acetic acid / 0.25 h / 16 - 20 °C / Inert atmosphere

2.1: hydrogenchloride; sodium hydroxide; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere

2.2: 1.75 h / 40 - 90 °C / Inert atmosphere

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; bromine; N,N-dimethyl-formamide; sodium hydroxide; sodium nitrite; In dichloromethane; water; acetic acid;
DOI:10.1002/anie.201106786