Technology Process of N-((1R,2S)-1-chloro-1-phenylpent-4-en-2-yl)-4-methylbenzenesulfonamide
There total 1 articles about N-((1R,2S)-1-chloro-1-phenylpent-4-en-2-yl)-4-methylbenzenesulfonamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(2S,3S)-2-allyl-3-phenyl-1-tosylaziridine;
With
boron trifluoride diethyl etherate; N-benzyl-N,N,N-triethylammonium chloride;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
With
water;
In
dichloromethane;
optical yield given as %de;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1021/jo902244y
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium cyanoborohydride;
In
tert-butyl alcohol;
at 85 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jo902244y
