p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

Base Information

Chemical Name:p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester
CAS No.:155908-77-3
Molecular Formula:C₂₁H₂₀ClNO₃S
Molecular Weight:401.914
Hs Code.:

Synonyms:p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

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Chemical Property of p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

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Technology Process of p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

There total 1 articles about p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77629-83-5,77053-56-6
ethyl 2-bromo-2-(4-methoxyphenyl) acetate

: 91166-79-9
bis(4-chloro-2-N-pyrrolylphenyl)disulfide

: 155908-77-3
p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) EtOH, reflux, 2.) EtOH, RT, 8 h;
DOI:10.1021/jm00036a007

Reference yield: 74.3%

: 155908-77-3
p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

: 155908-82-0
p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; ethanol; for 1h; Ambient temperature;
DOI:10.1021/jm00036a007

Reference yield:

: 155908-77-3
p-methoxy-α-<<4-chloro-2-(1H-pyrrol-1-yl)phenyl>thio>phenylacetic acid ethyl ester

: 155908-91-1
2-chloro-6-(p-methoxyphenyl)pyrrolo<2,1-d><1,5>benzothiazepin-7(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 74.3 percent / aq. NaOH / ethanol; tetrahydrofuran / 1 h / Ambient temperature

2: 43.5 percent / PCl₅ / CH₂Cl₂ / 5 h / 70 °C

With sodium hydroxide; phosphorus pentachloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00036a007