2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

• Chemical Name: 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside
• CAS No.: 911371-35-2
• Molecular Formula: C₇₈H₈₂O₁₈
• Molecular Weight: 1307.5

Synonyms:2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Chemical Property of 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 1 articles about 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2'-(benzyloxycarbonyl)benzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside → 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside (911371-35-2)

Guidance literature:

With ammonium acetate; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; at 20 ℃; for 1h;

DOI:10.1021/ol061444o

Reference yield: 45.0%

C59H94F3NO10S + 2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside (911371-35-2) → C128H169NO23 + C128H169NO23

Guidance literature:

With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; In dichloromethane; at -78 - 0 ℃; for 2h;

DOI:10.1021/ol061444o

Reference yield:

2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside (911371-35-2) → (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranosyl fluoride + (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl fluoride

Guidance literature:

2'-carboxybenzyl (2,3,5,6-tetra-O-benzyl-α-D-galactofuranosyl)-(1->2)-(3-O-benzyl-5,6-O-isopropylidene-β-D-galactofuranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; In dichloromethane; at -78 ℃;

With pyridine; hydrogen fluoride; In dichloromethane; at -78 - 0 ℃; for 2h;

DOI:10.1021/ol061444o

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