t-butyldiazaenyl benzoic acid

Base Information

• Chemical Name: t-butyldiazaenyl benzoic acid
• CAS No.: 521278-08-0
• Molecular Formula: C₁₂H₁₆N₂O₂S
• Molecular Weight: 252.337
• Mol file: 521278-08-0.mol

Synonyms:t-butyldiazaenyl benzoic acid

Chemical Property of t-butyldiazaenyl benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of t-butyldiazaenyl benzoic acid

There total 2 articles about t-butyldiazaenyl benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

3-amino-p-toluic acid (2458-12-0) + sodium tert-butyl thiolate (29364-29-2) → t-butyldiazaenyl benzoic acid (521278-08-0)

Guidance literature:

3-amino-p-toluic acid; With hydrogenchloride; sodium nitrite; In water; for 0.5h;

With sodium acetate; In water; pH=6;

sodium tert-butyl thiolate; In water; for 2h;

Reference yield:

C8H7N2O2(1+)*Cl(1-) (101333-46-4) + sodium tert-butyl thiolate (29364-29-2) → t-butyldiazaenyl benzoic acid (521278-08-0)

Guidance literature:

With sodium acetate; In water; for 2h; pH=6;

Reference yield:

t-butyldiazaenyl benzoic acid (521278-08-0) → 1H-indazole-6-carboxylic acid (704-91-6)

Guidance literature:

t-butyldiazaenyl benzoic acid; With potassium tert-butylate; In dimethyl sulfoxide; for 6h;

With hydrogenchloride; In water; dimethyl sulfoxide; at 0 ℃; pH=5 - 6;

upstream raw materials:

C₈H₇N₂O₂⁽¹⁺⁾*Cl^(1-)

sodium tert-butyl thiolate

3-amino-p-toluic acid

Downstream raw materials:

1H-indazole-6-carboxylic acid