C₁₄H₁₇NO₅

Base Information

Chemical Name:C₁₄H₁₇NO₅
CAS No.:1464782-15-7
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:

C<sub>14</sub>H<sub>17</sub>NO<sub>5</sub>

Synonyms:C₁₄H₁₇NO₅

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Chemical Property of C₁₄H₁₇NO₅

Chemical Property:

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Technology Process of C₁₄H₁₇NO₅

There total 6 articles about C₁₄H₁₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1464781-92-7
C₁₄H₁₅NO₄

: 1464782-15-7
C₁₄H₁₇NO₅

Guidance literature:: C₁₄H₁₅NO₄; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;

With sodium perborate; water; for 12h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c3cc45099f

Reference yield:

: 1033408-76-2
C₁₄H₂₅NO₄

: 1464782-15-7
C₁₄H₁₇NO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / -78 °C / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere

2.1: triethylamine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

3.1: acetic acid / water / 1 h / 80 °C / Inert atmosphere

4.1: C₂₅H₃₀Cl₂CuN₂O₂; N,N'-dimethylbenzylamine / toluene / 5 h / 20 °C / Inert atmosphere

5.1: triethylamine / tetrahydrofuran; toluene / 24 h / 20 °C / Inert atmosphere

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

6.2: 12 h / Inert atmosphere; Cooling with ice

With 2,6-dimethylpyridine; N,N'-dimethylbenzylamine; trimethylsilyl trifluoromethanesulfonate; C₂₅H₃₀Cl₂CuN₂O₂; acetic acid; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1039/c3cc45099f

Reference yield:

: 1464782-02-2
C₉H₁₇NO₂

: 1464782-15-7
C₁₄H₁₇NO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

2.1: acetic acid / water / 1 h / 80 °C / Inert atmosphere

3.1: C₂₅H₃₀Cl₂CuN₂O₂; N,N'-dimethylbenzylamine / toluene / 5 h / 20 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran; toluene / 24 h / 20 °C / Inert atmosphere

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

5.2: 12 h / Inert atmosphere; Cooling with ice

With N,N'-dimethylbenzylamine; C₂₅H₃₀Cl₂CuN₂O₂; acetic acid; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1039/c3cc45099f