Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester

Base Information

• Chemical Name: Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester
• CAS No.: 149790-56-7
• Molecular Formula: C₂₅H₂₉BrO₅
• Molecular Weight: 489.406

Synonyms:Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester

Chemical Property of Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester

Chemical Property:

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Technology Process of Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester

There total 2 articles about Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

Acetic acid 2-(2-acetoxy-5-tert-butyl-benzyl)-6-bromo-4-tert-butyl-phenyl ester (149790-50-1) → Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester (149790-56-7)

Guidance literature:

With chromium(VI) oxide; acetic anhydride; at 60 ℃; for 1h;

DOI:10.1246/bcsj.66.828

Reference yield:

2-(3-bromo-5-t-butyl-2-hydroxybenzyl)-4-t-butylphenol (78077-40-4) → Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester (149790-56-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / 4 h / 100 °C

2: 67 percent / aq. CrO₃, acetic anhydride / 1 h / 60 °C

With chromium(VI) oxide; hydrogenchloride; acetic anhydride;

DOI:10.1246/bcsj.66.828

Reference yield:

Acetic acid 2-(2-acetoxy-5-tert-butyl-benzoyl)-6-bromo-4-tert-butyl-phenyl ester (149790-56-7) → 2-(3-bromo-5-t-butylsalicyloyl)-4-t-butylphenol (149790-61-4)

Guidance literature:

With sodium hydroxide; In methanol; at 50 ℃; for 8h;

DOI:10.1246/bcsj.66.828

upstream raw materials:

Acetic acid 2-(2-acetoxy-5-tert-butyl-benzyl)-6-bromo-4-tert-butyl-phenyl ester

2-(3-bromo-5-t-butyl-2-hydroxybenzyl)-4-t-butylphenol

Downstream raw materials:

2-(3-bromo-5-t-butylsalicyloyl)-4-t-butylphenol

2-bromo-4-t-butyl-6-(5-t-butyl-3-chloromethylsalicyloyl)phenol

2-bromo-4-t-butyl-6-<5-t-butyl-3-(5-t-butylsalicyl)salicyloyl>phenol

2-bromo-4-t-butyl-6-<5-t-butyl-3-<5-t-butyl-3-(5-t-butylsalicyl)salicyl>salicyloyl>phenol

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