(4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

Base Information

Chemical Name:(4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid
CAS No.:138962-84-2
Molecular Formula:C₁₇H₁₃N₃O₂S₂
Molecular Weight:355.441
Hs Code.:

Synonyms:(4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

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Chemical Property of (4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

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Technology Process of (4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

There total 2 articles about (4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 138962-90-0
4-Phenyl-2,4-dihydro-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene-1-thione

: 79-11-8
chloroacetic acid

: 138962-84-2
(4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

Guidance literature:: With potassium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; for 15h; Ambient temperature;
DOI:10.1016/0223-5234(91)90011-B

Reference yield:

: 130336-92-4
C₂₁H₁₈N₄S₂

: 138962-84-2
(4-Phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalen-1-ylsulfanyl)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / dimethylformamide / 2 h / Heating

2: 73 percent / TBAB, KOH / tetrahydrofuran / 15 h / Ambient temperature

With potassium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(91)90011-B