(1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate

Base Information

• Chemical Name: (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate
• CAS No.: 29364-08-7
• Molecular Formula: C₁₇H₂₂N₂O₄
• Molecular Weight: 318.373

Synonyms:(1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate

Chemical Property of (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate

There total 4 articles about (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.3%

phenyl isocyanate (103-71-9) + methyl ecgonine (7143-09-1) → (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate (29364-08-7)

Guidance literature:

In toluene; for 2h; Heating;

DOI:10.1021/jm00106a035

Reference yield:

(-)-cocaine hydrochloride (53-21-4) → (1R-2-exo-3-exo)-2-carbomethoxy-8-methyl-8-azabicyclo<3.2.1>octyl-3-N-phenylcarbamate (29364-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent

2: 58.3 percent / toluene / 2 h / Heating

In toluene;

DOI:10.1021/jm00106a035

Reference yield:

→ (1R,2S,3S,5R)-8-Methyl-3-phenylcarbamoyloxy-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid methyl ester (29364-08-7)

Guidance literature:

Pseudoecgoninmethylester, Phenylisocyanat;

upstream raw materials:

phenyl isocyanate

methyl ecgonine

(-)-cocaine hydrochloride

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