cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

Base Information

Chemical Name:cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)
CAS No.:235779-96-1
Molecular Formula:C₂₄H₄₂N₂O₆
Molecular Weight:454.607
Hs Code.:

Synonyms:cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

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Technology Process of cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

There total 2 articles about cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 15753-50-1,25712-33-8
cis-1,2-cyclohexanedimethanol

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 235779-96-1
cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

Guidance literature:: cis-1,2-cyclohexanedimethanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride; In tetrahydrofuran; for 16h; Heating;
DOI:10.1002/(SICI)1521-3765(19990604)5:6<1905::AID-CHEM1905>3.0.CO;2-4

Reference yield:

: 235780-27-5
cis-1,2-Cyclohexanedimethyl bis[N-(2-hydroxy-1,1-dimethylethyl)carbamate]

: 235779-96-1
cis-1,2-Cyclohexanedimethyl bis(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / K₂CO₃; MeOH / 3 h / Heating

2.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

2.2: 88 percent / tetrahydrofuran / 16 h / Heating

With methanol; sodium hydride; potassium carbonate; In tetrahydrofuran; 1.1: deacylation / 2.1: Metallation / 2.2: Acylation;
DOI:10.1002/(SICI)1521-3765(19990604)5:6<1905::AID-CHEM1905>3.0.CO;2-4