2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione

Base Information

• Chemical Name: 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione
• CAS No.: 72708-78-2
• Molecular Formula: C₂₃H₁₇N₃O₄
• Molecular Weight: 399.406
• Mol file: 72708-78-2.mol

Synonyms:2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione

Chemical Property of 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione

There total 1 articles about 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 1,3-diphenylpropanedione (120-46-7,61346-73-4) → 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione (72708-78-2)

Guidance literature:

In tetrahydrofuran;

DOI:10.1021/jo01295a014

Reference yield: 69.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione (72708-78-2) → 2,2-Bis(4-phenylurazolyl)-1,3-diphenyl-1,3-propanedione (72708-79-3)

Guidance literature:

In dichloromethane; for 144h; Ambient temperature;

DOI:10.1021/jo00288a032

Reference yield:

2-(4-Phenyl-2H-1,2,4-triazoline-3,5-dionyl)-1,3-diphenyl-1,3-propanedione (72708-78-2) → C23H15N3O4

Guidance literature:

With tert-butylhypochlorite; In tetrahydrofuran; for 0.0166667h;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

1,3-diphenylpropanedione

Downstream raw materials:

2,2-Bis(4-phenylurazolyl)-1,3-diphenyl-1,3-propanedione

1,3-diphenyl-propane-1,2,3-trione

tetrabenzoylethylene

2-(4,4-dimethyl-2,6-dioxo-3,5-dioxan-1-ylidene)-1,3-diphenyl-1,3-propanedione