methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

Base Information

Chemical Name:methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate
CAS No.:1204414-22-1
Molecular Formula:C₂₀H₂₄BNO₅S
Molecular Weight:401.291
Hs Code.:

Synonyms:methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

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Chemical Property of methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

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Technology Process of methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

There total 1 articles about methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 39098-97-0
2-thienylacetic acid chloride

: 524916-42-5
methyl 4-amino-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 1204414-22-1
methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo901930v

Reference yield: 81.0%

: 1204414-22-1
methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate

: 1204414-34-5
methyl 3-(difluoroboryl)-4-[(2-thienylacetyl)amino]benzoate

Guidance literature:: methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-[(2-thienylacetyl)amino]benzoate; With potassium hydrogenfluoride; In methanol; water; at 20 ℃; for 1h;

With water; for 16h;
DOI:10.1021/jo901930v