C₆₄H₁₀₀N₃O₂₂PS₂

Base Information

Chemical Name:C₆₄H₁₀₀N₃O₂₂PS₂
CAS No.:1310568-66-1
Molecular Formula:C₆₄H₁₀₀N₃O₂₂PS₂
Molecular Weight:1358.61
Hs Code.:

C<sub>64</sub>H<sub>100</sub>N<sub>3</sub>O<sub>22</sub>PS<sub>2</sub>

Synonyms:C₆₄H₁₀₀N₃O₂₂PS₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₁₀₀N₃O₂₂PS₂

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Technology Process of C₆₄H₁₀₀N₃O₂₂PS₂

There total 15 articles about C₆₄H₁₀₀N₃O₂₂PS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: patent blue VF sulfonyl chloride

: 1310568-65-0
C₃₇H₇₀NO₁₇P

: 1310568-66-1
C₆₄H₁₀₀N₃O₂₂PS₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 1310568-59-2
C₂₈H₄₇BrO₁₁

: 1310568-66-1
C₆₄H₁₀₀N₃O₂₂PS₂

Guidance literature:: Multi-step reaction with 5 steps

1: 2 h / 160 °C

2: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

3: potassium carbonate; potassium iodide / acetone / 48 h / 60 °C

4: trifluoroacetic acid / dichloromethane / 0 - 20 °C

5: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 3: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 1310568-58-1
C₂₈H₄₈O₁₂

: 1310568-66-1
C₆₄H₁₀₀N₃O₂₂PS₂

Guidance literature:: Multi-step reaction with 6 steps

1: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C

2: 2 h / 160 °C

3: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

4: potassium carbonate; potassium iodide / acetone / 48 h / 60 °C

5: trifluoroacetic acid / dichloromethane / 0 - 20 °C

6: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; potassium carbonate; triethylamine; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 4: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144