1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

Base Information

Chemical Name:1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene
CAS No.:1061586-97-7
Molecular Formula:C₂₃H₄₁IO₂Si₃
Molecular Weight:560.738
Hs Code.:

Synonyms:1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

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Technology Process of 1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

There total 1 articles about 1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 4,5-bis(tert-butyldimethylsilyloxy)-1,2-diiodobenzene

: 1066-54-2
trimethylsilylacetylene

: 1061586-97-7
1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/b806444j

Reference yield: 94.0%

: 1061586-97-7
1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

: 1061586-98-8
1,2-bis(tert-butyldimethylsiloxy)-4-ethynyl-5-iodobenzene

Guidance literature:: With pyridine; silver nitrate; In water; acetone; at 50 ℃; for 48h; Inert atmosphere;
DOI:10.1039/b806444j

Reference yield: 82.0%

: 1061586-97-7
1,2-bis(tert-butyldimethylsiloxy)-4-iodo-5-[(trimethylsilyl)ethynyl]benzene

: C₄₀H₆₅BrO₄Si₄

: C₆₃H₁₀₅BrO₆Si₇

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; at 23 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jacs.6b10316