3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

Base Information

Chemical Name:3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine
CAS No.:1454333-40-4
Molecular Formula:C₃₀H₄₅IN₂O₈Si
Molecular Weight:716.686
Hs Code.:

Synonyms:3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

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Chemical Property of 3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

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Technology Process of 3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

There total 2 articles about 3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1408078-57-8
2-[(1-methyl)vinyloxy]ethyl benzoate

: 129696-31-7
5-iodo-5′-O-triisopropylsilyl-2′-deoxyuridine

: 1454333-40-4
3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

Guidance literature:: With camphor-10-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1039/c3ob41428k

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1454333-40-4
3’-O-(1-(2-(benzoyloxy)ethoxy)-1-methylethyl)-5-iodo-5’-O-triisopropylsilyl-2’-deoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 19 h / 0 - 20 °C

2: camphor-10-sulfonic acid / tetrahydrofuran / 4 h / 20 °C

With 1H-imidazole; dmap; camphor-10-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41428k