2-phenyl-2-(pyridazin-4-yl)ethanamine

Base Information

Chemical Name:2-phenyl-2-(pyridazin-4-yl)ethanamine
CAS No.:1598429-41-4
Molecular Formula:C₁₂H₁₃N₃
Molecular Weight:199.255
Hs Code.:

Synonyms:2-phenyl-2-(pyridazin-4-yl)ethanamine

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Chemical Property of 2-phenyl-2-(pyridazin-4-yl)ethanamine

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Technology Process of 2-phenyl-2-(pyridazin-4-yl)ethanamine

There total 8 articles about 2-phenyl-2-(pyridazin-4-yl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1600499-20-4
tert-butyl (2-phenyl-2-(pyridazin-4-yl)ethyl)carbamate

: 1598429-41-4
2-phenyl-2-(pyridazin-4-yl)ethanamine

Guidance literature:: tert-butyl (2-phenyl-2-(pyridazin-4-yl)ethyl)carbamate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

With sodium carbonate; In water; pH=9-10;

Reference yield:

: 53074-22-9
4-benzylpyridazine

: 1598429-41-4
2-phenyl-2-(pyridazin-4-yl)ethanamine

Guidance literature:: Multi-step reaction with 7 steps

1.1: selenium(IV) oxide; acetic acid / 1 h / 100 °C

2.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C

2.2: 4 h / 0 °C

3.1: benzenesufonyl hydrazide; triethylamine / toluene / 100 °C

4.1: sodium hydroxide; water / methanol

4.2: pH 4-5

5.1: diphenyl phosphoryl azide; triethylamine / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

6.1: toluene / 80 °C

7.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

7.2: pH 9-10

With selenium(IV) oxide; diphenyl phosphoryl azide; water; sodium hydride; acetic acid; triethylamine; benzenesufonyl hydrazide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 103-82-2
phenylacetic acid

: 1598429-41-4
2-phenyl-2-(pyridazin-4-yl)ethanamine

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; silver nitrate; ammonium persulfate / water / 1.5 h / 60 - 90 °C

2.1: selenium(IV) oxide; acetic acid / 1 h / 100 °C

3.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C

3.2: 4 h / 0 °C

4.1: benzenesufonyl hydrazide; triethylamine / toluene / 100 °C

5.1: sodium hydroxide; water / methanol

5.2: pH 4-5

6.1: diphenyl phosphoryl azide; triethylamine / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

7.1: toluene / 80 °C

8.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

8.2: pH 9-10

With selenium(IV) oxide; ammonium persulfate; sulfuric acid; diphenyl phosphoryl azide; water; sodium hydride; silver nitrate; acetic acid; triethylamine; benzenesufonyl hydrazide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;