C₃₅H₆₄O₆Si₂

Base Information

Chemical Name:C₃₅H₆₄O₆Si₂
CAS No.:1355239-70-1
Molecular Formula:C₃₅H₆₄O₆Si₂
Molecular Weight:637.061
Hs Code.:

C<sub>35</sub>H<sub>64</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₅H₆₄O₆Si₂

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Chemical Property of C₃₅H₆₄O₆Si₂

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Technology Process of C₃₅H₆₄O₆Si₂

There total 12 articles about C₃₅H₆₄O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1355240-14-0
C₃₅H₆₆O₆Si₂

: 1355239-70-1
C₃₅H₆₄O₆Si₂

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 35 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol203342e

Reference yield:

: 1355240-03-7
C₁₄H₁₈O₂

: 1355239-70-1
C₃₅H₆₄O₆Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

1.2: 0.17 h / -78 - 0 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -78 °C / Inert atmosphere

2.2: -78 - 25 °C / Inert atmosphere

2.3: 4 h / 20 - 25 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

4.2: 1 h / -78 - 0 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 2.33 h / -78 °C / Inert atmosphere

5.2: 4 h / -78 - 0 °C / Inert atmosphere

5.3: Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

7.2: 2 h / -78 °C / Inert atmosphere

8.1: potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / tert-butyl alcohol / 60 h / 0 °C / Inert atmosphere

9.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 48 h / 35 °C / Inert atmosphere

With 1H-imidazole; potassium osmate(VI) dihydrate; n-butyllithium; zirconocene dichloride; methanesulfonamide; water; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; mineral oil; tert-butyl alcohol; pentane; 8.1: Sharpless dihydroxylation / 9.1: Parikh-Doering oxidation;
DOI:10.1021/ol203342e

Reference yield:

: 1355240-06-0
C₁₄H₁₉IO₂

: 1355239-70-1
C₃₅H₆₄O₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -78 °C / Inert atmosphere

1.2: -78 - 25 °C / Inert atmosphere

1.3: 4 h / 20 - 25 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

3.2: 1 h / -78 - 0 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2.33 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 - 0 °C / Inert atmosphere

4.3: Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

6.2: 2 h / -78 °C / Inert atmosphere

7.1: potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / tert-butyl alcohol / 60 h / 0 °C / Inert atmosphere

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 48 h / 35 °C / Inert atmosphere

With 1H-imidazole; potassium osmate(VI) dihydrate; n-butyllithium; methanesulfonamide; water; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; mineral oil; tert-butyl alcohol; pentane; 7.1: Sharpless dihydroxylation / 8.1: Parikh-Doering oxidation;
DOI:10.1021/ol203342e