(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Base Information

Chemical Name:(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside
CAS No.:179924-49-3
Molecular Formula:C₅₉H₅₄O₆
Molecular Weight:859.074
Hs Code.:

Synonyms:(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Suppliers and Price of (R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

There total 7 articles about (R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76-83-5
trityl chloride

: 179924-48-2
(R)-2-hydroxy-1-phenylethyl-3-O-benzyl-2-deoxy-L-glucoside

: 179924-49-3
(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Guidance literature:: In pyridine; at 20 ℃; for 96h;
DOI:10.1002/(SICI)1099-0690(199911)1999:11<2885::AID-EJOC2885>3.0.CO;2-J

Reference yield:

: 179924-43-7
methyl trans-4-benzyloxy-2-oxo-3-butenoate

: 179924-49-3
(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Eu(fod)3 / petroleum ether; toluene / Heating

1.2: LiAlH₄ / diethyl ether / 15 h / 20 °C

1.3: BH₃*Me₂S / tetrahydrofuran / 40 h / 20 °C

2.1: 85 percent / pyridine / 96 h / 20 °C

With Eu(fod)3; In pyridine; toluene; Petroleum ether; 1.1: Cyclization / 1.2: Reduction / 1.3: Addition / 2.1: Alkylation;
DOI:10.1002/(SICI)1099-0690(199911)1999:11<2885::AID-EJOC2885>3.0.CO;2-J

Reference yield:

: 164386-44-1
(R)-Phenyl-vinyloxy-acetic acid butyl ester

: 179924-49-3
(R)-1-phenyl-2-(α,α-diphenylbenzyloxy)ethyl-3-O-benzyl-2-deoxy-6-O-(α,α-diphenylbenzyl)-L-glucoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Eu(fod)3 / petroleum ether; toluene / Heating

1.2: LiAlH₄ / diethyl ether / 15 h / 20 °C

1.3: BH₃*Me₂S / tetrahydrofuran / 40 h / 20 °C

2.1: 85 percent / pyridine / 96 h / 20 °C

With Eu(fod)3; In pyridine; toluene; Petroleum ether; 1.1: Cyclization / 1.2: Reduction / 1.3: Addition / 2.1: Alkylation;
DOI:10.1002/(SICI)1099-0690(199911)1999:11<2885::AID-EJOC2885>3.0.CO;2-J