N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

Base Information

Chemical Name:N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine
CAS No.:927804-14-6
Molecular Formula:C₄₁H₅₂N₄
Molecular Weight:600.891
Hs Code.:

Synonyms:N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

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Chemical Property of N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

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Technology Process of N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

There total 1 articles about N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 927804-09-9
N,N'-bis[(2-fluorophenyl)methylene]-1,3-propanediamine

: 927804-14-6
N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

Guidance literature:: 2,6-diisopropylbenzenamine; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 12h;

N,N'-bis[(2-fluorophenyl)methylene]-1,3-propanediamine; In tetrahydrofuran; at -35 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.02.003

Reference yield: 82.0%

: 927804-14-6
N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

: 75-24-1
trimethylaluminum

: 1370530-01-0
[(AlMe₂)2(N,N'-bis[2-(2,6-diisopropylphenylamino)benzylidene]-1,3-propanediamine)]

Guidance literature:: In n-heptane; toluene; toluene soln. of ligand added dropwise to heptane soln. of Al compd. (1:1 molar ratio), stirred, sealed (N2), stirred at 110°C for 24 h; evapd., washed (pentane), elem. anal.;
DOI:10.1016/j.jorganchem.2012.02.003

Reference yield: 57.0%

: 927804-14-6
N,N'-bis[(2-(2,6-diisopropylphenylamino)benzylidene)]-1,3-propanediamine

: 557-20-0
diethylzinc

: 927804-16-8
[Zn₂(C₂H₅)2((CH₂)3(NCHC₆H₄NC₆H₃(CH(CH₃)2)2)2)]

Guidance literature:: In toluene; pentane; byproducts: C2H6; using Schlenk techniques; addn. of ZnEt2 (2 equiv.) to soln. of (CH2)3(NCHC6H4NHC6H3(CHMe2)2)2 (1 equiv.) in toluene-pentane (50:50) at 0°C; stirring at room temp. for 12 h; concn. under reduced presure, standing at -25°C for 12 h; crystn., elem. anal.;
DOI:10.1039/b615080b