(S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide

Base Information

• Chemical Name: (S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide
• CAS No.: 737777-08-1
• Molecular Formula: C₂₃H₂₅NO₂S₂
• Molecular Weight: 411.589

Synonyms:(S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide

Chemical Property of (S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide

Chemical Property:

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Technology Process of (S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide

There total 2 articles about (S)-N-[(1S,S_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

(S)-methyl p-tolyl sulfoxide (5056-07-5) + [S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide (65440-68-8) → (S)-N-[(1S,Ss)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide (737777-08-1)

Guidance literature:

(S)-methyl p-tolyl sulfoxide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

[S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide; In tetrahydrofuran; hexane; at 0 ℃; for 24h;

DOI:10.1021/jo049666s

Reference yield:

(S)-methyl p-tolyl sulfoxide (5056-07-5) + [S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide (65440-68-8) → (S)-N-[(1R,Ss)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide + (S)-N-[(1S,Ss)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide (737777-08-1)

Guidance literature:

(S)-methyl p-tolyl sulfoxide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

[S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide; In tetrahydrofuran; hexane; at -78 ℃; for 24h;

DOI:10.1021/jo049666s

Reference yield: 90.0%

(S)-N-[(1S,Ss)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]-p-toluenesulfinamide (737777-08-1) → (1S,Rs)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethylamine (737777-23-0)

Guidance literature:

With trifluoroacetic acid; In methanol; at 0 ℃; for 3h;

DOI:10.1021/jo049666s

upstream raw materials:

(S)-methyl p-tolyl sulfoxide

[S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide

Downstream raw materials:

(1S,R_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethylamine

trifluoro-acetic acid 2-tert-butoxycarbonylamino-2-phenyl-propyl ester

tert-butyl N-[(1S,R_s)-1-methyl-1-phenyl-2-(p-tolylsulfinyl)ethyl]carbamate

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