(2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

Base Information

Chemical Name:(2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate
CAS No.:1436866-57-7
Molecular Formula:C₁₃H₉F₃N₂O₃S₂
Molecular Weight:362.353
Hs Code.:

Synonyms:(2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

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Chemical Property of (2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

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Technology Process of (2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

There total 2 articles about (2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4900-99-6
2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-ol

: 358-23-6
trifluoromethylsulfonic anhydride

: 1436866-57-7
(2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1016/j.bmcl.2013.03.104

Reference yield:

: 2689-69-2
methyl tetrahydrothiophen-3-one-2-carboxylate

: 1436866-57-7
(2-phenyl-6,7-dihydrothieno[3,2-d]pyrimidin-4-yl) trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 18 h / 20 - 85 °C

2: triethylamine / dichloromethane / 15 h / 0 - 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.03.104