5,10-diphenyl-16-N-methyltripyrrane

Base Information

• Chemical Name: 5,10-diphenyl-16-N-methyltripyrrane
• CAS No.: 237081-19-5
• Molecular Formula: C₂₇H₂₅N₃
• Molecular Weight: 391.516
• Mol file: 237081-19-5.mol

Synonyms:5,10-diphenyl-16-N-methyltripyrrane

Chemical Property of 5,10-diphenyl-16-N-methyltripyrrane

Chemical Property:

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Technology Process of 5,10-diphenyl-16-N-methyltripyrrane

There total 1 articles about 5,10-diphenyl-16-N-methyltripyrrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

pyrrole (109-97-7,30604-81-0) + 2,5-bis(phenylhydroxymethyl)-N-methylpyrrole → 5,10-diphenyl-16-N-methyltripyrrane (237081-19-5)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 0.5h;

DOI:10.1039/a900137i

Reference yield: 26.0%

5,10-diphenyl-16-N-methyltripyrrane (237081-19-5) + 5,5'-bis-(phenylhydroxymethyl)-2,2'-biselenophene (238079-40-8) → 5,10,15,20-tetraphenyl-27-N-methyl-25,29-diselenasapphyrin

Guidance literature:

5,10-diphenyl-16-N-methyltripyrrane; 5,5'-bis-(phenylhydroxymethyl)-2,2'-biselenophene; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With air; chloranil; In dichloromethane; for 1h; Heating;

DOI:10.1021/jo990729u

Reference yield: 26.0%

5,5′-bis(phenylhydroxymethyl)-2,2′-bithiophene (201858-09-5) + 5,10-diphenyl-16-N-methyltripyrrane (237081-19-5) → 5,10,15,20-tetraphenyl-27-N-methyl-25,29-dithiasapphyrin

Guidance literature:

5,5′-bis(phenylhydroxymethyl)-2,2′-bithiophene; 5,10-diphenyl-16-N-methyltripyrrane; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With chloranil; In dichloromethane; Heating;

DOI:10.1039/a900137i

upstream raw materials:

pyrrole