N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

Base Information

Chemical Name:N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide
CAS No.:1579294-14-6
Molecular Formula:C₂₅H₃₄N₂O₄
Molecular Weight:426.556
Hs Code.:

Synonyms:N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

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Chemical Property of N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

Chemical Property:

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Technology Process of N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

There total 6 articles about N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1579295-31-0
methyl 2-(4-(4-(4-(3-morpholinopropoxy)phenyl)butyl)phenyl)acetate

: 1579294-14-6
N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

Guidance literature:: With hydroxylamine; sodium methylate; In methanol; water; at 0 - 20 ℃; for 4.5h; Inert atmosphere;

Reference yield:

: 1579295-30-9
methyl 2-(4-(4-(4-hydroxyphenyl)butyl)phenyl)acetate

: 1579294-14-6
N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide; potassium carbonate / N,N-dimethyl-formamide; water / 20 - 55 °C / Inert atmosphere

2: sodium methylate; hydroxylamine / methanol; water / 4.5 h / 0 - 20 °C / Inert atmosphere

With hydroxylamine; sodium methylate; potassium carbonate; sodium iodide; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1035211-53-0
methyl 2-(4-(but-3-ynyl)phenyl)acetate

: 1579294-14-6
N-hydroxy-2-(4-(4-(4-(3-morpholinopropoxy) phenyl)butyl)phenyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; N-ethyl-N,N-diisopropylamine / 1,2-dimethoxyethane / 18 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 17 h / 20 °C

3: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: sodium iodide; potassium carbonate / N,N-dimethyl-formamide; water / 20 - 55 °C / Inert atmosphere

5: sodium methylate; hydroxylamine / methanol; water / 4.5 h / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; hydroxylamine; sodium methylate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;