Technology Process of C24H26N2O3
There total 8 articles about C24H26N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C25H28N2O3;
With
water; sodium hydroxide;
In
methanol;
at 60 ℃;
for 3h;
With
water; ammonium chloride;
In
methanol;
Saturated solution;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aluminum (III) chloride / dichloromethane
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide
3: water; sodium hydroxide / tetrahydrofuran; methanol
With
aluminum (III) chloride; water; potassium carbonate; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml100184k
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
3.1: acetic acid / 8 h / 80 °C
3.2: 18 h / 90 °C / Reflux
4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h
4.2: 2 h
5.1: aluminum (III) chloride / dichloromethane / 7 h / 20 °C / Inert atmosphere
6.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere
7.1: water; sodium hydroxide / methanol / 3 h / 60 °C
7.2: Saturated solution
With
hydrogenchloride; aluminum (III) chloride; water; hydrogen; sodium hydride; potassium carbonate; acetic acid; potassium iodide; sodium hydroxide;
palladium on activated charcoal;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
