3',4'-difluoro-2'-(2-oxopropyl)-anilide

Base Information

Chemical Name:3',4'-difluoro-2'-(2-oxopropyl)-anilide
CAS No.:146617-77-8
Molecular Formula:C₂₁H₂₂F₂N₂O₄S
Molecular Weight:436.479
Hs Code.:

3',4'-difluoro-2'-(2-oxopropyl)-<N-p-toluenesulfonyl-(R)-prolin>anilide

Synonyms:3',4'-difluoro-2'-(2-oxopropyl)-anilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3',4'-difluoro-2'-(2-oxopropyl)-anilide

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Technology Process of 3',4'-difluoro-2'-(2-oxopropyl)-anilide

There total 3 articles about 3',4'-difluoro-2'-(2-oxopropyl)-anilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3',4'-difluoro-2'-(2-hydroxypropyl)-anilide

: 146617-77-8
3',4'-difluoro-2'-(2-oxopropyl)-anilide

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetone; for 0.75h; Ambient temperature;
DOI:10.1248/cpb.43.1678

Reference yield:

: 121247-18-5
3,4-difluoro-2-(2-hydroxypropyl)aniline

: 146617-77-8
3',4'-difluoro-2'-(2-oxopropyl)-anilide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / CH₂Cl₂ / 0.5 h / -5 °C

2: 100 percent / CrO₃, 30percent aq. H₂SO₄ / acetone / 0.75 h / Ambient temperature

With pyridine; chromium(VI) oxide; sulfuric acid; In dichloromethane; acetone;
DOI:10.1248/cpb.43.1678

Reference yield:

: 118776-39-9
(2R)-(+)-1-(4-toluenesulphonyl)prolyl chloride

: 146617-77-8
3',4'-difluoro-2'-(2-oxopropyl)-anilide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / CH₂Cl₂ / 0.5 h / -5 °C

2: 100 percent / CrO₃, 30percent aq. H₂SO₄ / acetone / 0.75 h / Ambient temperature

With pyridine; chromium(VI) oxide; sulfuric acid; In dichloromethane; acetone;
DOI:10.1248/cpb.43.1678