butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

Base Information

Chemical Name:butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate
CAS No.:1355019-92-9
Molecular Formula:C₂₉H₃₀N₂O₄S
Molecular Weight:502.634
Hs Code.:

Synonyms:butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

Suppliers and Price of butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

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Technology Process of butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

There total 2 articles about butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 1355019-77-0
N-(2-(1H-indol-1-yl)-4-methylphenyl)-4-methylbenzenesulfonamide

: 1355019-92-9
butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

Guidance literature:: With lithium acetate; copper diacetate; sodium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 110 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol203275b

Reference yield:

: 1224955-12-7
2-(1H-indol-1-yl)-4-methylaniline

: 98-59-9
p-toluenesulfonyl chloride

: 1355019-92-9
butyl 2-(2-methyl-5-tosyl-5,6-dihydroindolo[1,2-a]quinoxalin-6-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Inert atmosphere; Reflux

2: lithium acetate; copper diacetate; sodium acetate; palladium diacetate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

With pyridine; lithium acetate; copper diacetate; sodium acetate; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1021/ol203275b