C₂₂H₃₀O₂

Base Information

Chemical Name:C₂₂H₃₀O₂
CAS No.:1361399-06-5
Molecular Formula:C₂₂H₃₀O₂
Molecular Weight:326.479
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>2</sub>

Synonyms:C₂₂H₃₀O₂

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Chemical Property of C₂₂H₃₀O₂

Chemical Property:

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Technology Process of C₂₂H₃₀O₂

There total 7 articles about C₂₂H₃₀O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1361399-05-4
C₂₄H₃₆O₂

: 1361399-06-5
C₂₂H₃₀O₂

Guidance literature:: With ammonium cerium (IV) nitrate; In dichloromethane; water; acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1021/ol300257v

Reference yield:

: 1361399-02-1
C₂₃H₃₆O₄

: 1361399-06-5
C₂₂H₃₀O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / -78 - 20 °C

2.1: iodine; magnesium / diethyl ether / 0.5 h / Reflux

2.2: 24 h / 0 - 20 °C

3.1: toluene-4-sulfonic acid / methanol / 16 h / 20 °C

4.1: ammonium cerium (IV) nitrate / dichloromethane; water; acetonitrile / 0.5 h / 0 °C

With ammonium cerium (IV) nitrate; iodine; toluene-4-sulfonic acid; magnesium; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane; water; acetonitrile; 1.1: Pinacol rearrangement;
DOI:10.1021/ol300257v

Reference yield:

: 1361399-03-2
C₂₃H₃₄O₃

: 1361399-06-5
C₂₂H₃₀O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; magnesium / diethyl ether / 0.5 h / Reflux

1.2: 24 h / 0 - 20 °C

2.1: toluene-4-sulfonic acid / methanol / 16 h / 20 °C

3.1: ammonium cerium (IV) nitrate / dichloromethane; water; acetonitrile / 0.5 h / 0 °C

With ammonium cerium (IV) nitrate; iodine; toluene-4-sulfonic acid; magnesium; In methanol; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1021/ol300257v