C₄₄H₄₇F₅O₁₆

Base Information

Chemical Name:C₄₄H₄₇F₅O₁₆
CAS No.:1449241-36-4
Molecular Formula:C₄₄H₄₇F₅O₁₆
Molecular Weight:926.84
Hs Code.:

C<sub>44</sub>H<sub>47</sub>F<sub>5</sub>O<sub>16</sub>

Synonyms:C₄₄H₄₇F₅O₁₆

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Chemical Property of C₄₄H₄₇F₅O₁₆

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Technology Process of C₄₄H₄₇F₅O₁₆

There total 3 articles about C₄₄H₄₇F₅O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1449241-35-3
C₃₁H₃₁F₅O₆S

: 18968-05-3
1,3,4,6-tetra-O-acetyl-β-D-mannopyranose

: 1449241-36-4
C₄₄H₄₇F₅O₁₆

Guidance literature:: C₃₁H₃₁F₅O₆S; 1,3,4,6-tetra-O-acetyl-β-D-mannopyranose; With 2,6-di-tert-butyl-4-methylpyridine; In 1,2-dichloro-ethane; for 0.5h; Inert atmosphere; Molecular sieve;

With methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 - 50 ℃; for 15.5h;
DOI:10.1002/anie.201301613

Reference yield:

: 1236054-94-6
methyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 1449241-36-4
C₄₄H₄₇F₅O₁₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride; hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 9 h / 0 °C / Molecular sieve

2.1: pyridine / dichloromethane / 1.5 h / 20 °C / Cooling with ice

3.1: 2,6-di-tert-butyl-4-methylpyridine / 1,2-dichloro-ethane / 0.5 h / Inert atmosphere; Molecular sieve

3.2: 15.5 h / 20 - 50 °C

With pyridine; hydrogenchloride; 2,6-di-tert-butyl-4-methylpyridine; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201301613

Reference yield:

: 1449241-34-2
C₂₈H₃₂O₅S

: 1449241-36-4
C₄₄H₄₇F₅O₁₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 1.5 h / 20 °C / Cooling with ice

2.1: 2,6-di-tert-butyl-4-methylpyridine / 1,2-dichloro-ethane / 0.5 h / Inert atmosphere; Molecular sieve

2.2: 15.5 h / 20 - 50 °C

With pyridine; 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201301613