3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

Base Information

Chemical Name:3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone
CAS No.:1105506-22-6
Molecular Formula:C₃₅H₄₂O₇
Molecular Weight:574.714
Hs Code.:

Synonyms:3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

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Chemical Property of 3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

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Technology Process of 3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

There total 1 articles about 3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 90-96-0
bis(p-methoxyphenyl)methanone

: 73448-14-3
hex-5-ynoic acid tert-butyl ester

: 845272-51-7
3-[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

: 1105506-22-6
3,3'-bis[5-(tert-butyloxycarbonyl)pent-1-ynyl]-4,4'-dimethoxybenzophenone

Guidance literature:: bis(p-methoxyphenyl)methanone; With N-iodo-succinimide; trifluoroacetic acid; In acetonitrile; for 5h; Heating;

hex-5-ynoic acid tert-butyl ester; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1039/b810600b