C₃₅H₄₇NO₅SSi

Base Information Edit

Chemical Name:C₃₅H₄₇NO₅SSi
CAS No.:114634-58-1
Molecular Formula:C₃₅H₄₇NO₅SSi
Molecular Weight:621.913
Hs Code.:
Mol file:114634-58-1.mol

C<sub>35</sub>H<sub>47</sub>NO<sub>5</sub>SSi

Synonyms:C₃₅H₄₇NO₅SSi

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Chemical Property of C₃₅H₄₇NO₅SSi Edit

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Technology Process of C₃₅H₄₇NO₅SSi

There total 10 articles about C₃₅H₄₇NO₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 127354-70-5
C₃₃H₄₅NO₄SSi

: 108-24-7
acetic anhydride

: 114634-58-1
C₃₅H₄₇NO₅SSi

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; for 144h; Ambient temperature;
DOI:10.1021/ja00167a037

Reference yield:

: 114634-56-9
C₃₂H₄₃NO₄SSi

: 114634-58-1
C₃₅H₄₇NO₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: DMAP, DBU / acetonitrile

2: LiN(SiMe₃)2 / tetrahydrofuran / -78 - -40 °C

3: HNEt₃F / tetrahydrofuran; methanol

4: DMAP, Et₃N / tetrahydrofuran

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine hydrofluoride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja00222a047

Reference yield:

: 114634-55-8
C₃₄H₄₅NO₅SSi

: 114634-58-1
C₃₅H₄₇NO₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / methanol / -15 °C

2: DMAP, DBU / acetonitrile

3: LiN(SiMe₃)2 / tetrahydrofuran / -78 - -40 °C

4: HNEt₃F / tetrahydrofuran; methanol

5: DMAP, Et₃N / tetrahydrofuran

With dmap; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine hydrofluoride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja00222a047