1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

Base Information

Chemical Name:1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)
CAS No.:1277182-11-2
Molecular Formula:C₂₅H₄₁N₇O₅
Molecular Weight:519.644
Hs Code.:

Synonyms:1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

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Chemical Property of 1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

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Technology Process of 1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

There total 1 articles about 1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 34680-81-4
2-bromo-N-methylacetamide

: 1-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecane trihydrochloride

: 1277182-11-2
1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

Guidance literature:: With potassium carbonate; In acetonitrile; at 65 - 70 ℃; for 12h;
DOI:10.1016/j.bmc.2010.06.026

Reference yield:

: 1277182-11-2
1-benzyloxycarbonyl-1,4,7,10-tetraazacyclododecane-4,7,10-tri(methylcarbonylamide)

: 1277182-13-4
C₂₈H₄₆N₈O₆

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 72 h / 2585.81 Torr

2: potassium carbonate / acetonitrile / 65 - 70 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2010.06.026