Technology Process of C34H74O6Si3
There total 7 articles about C34H74O6Si3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
toluene;
at 100 ℃;
DOI:10.1039/b700827a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere
1.2: 17 h / -78 - -20 °C / Inert atmosphere
2.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 21 h / -30 - -20 °C / Inert atmosphere
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / Molecular sieve; Inert atmosphere
4.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
5.1: dimethyl sulfide borane / toluene / 3 h / 100 °C / Inert atmosphere
With
2,6-dimethylpyridine; dimethyl sulfide borane; acetic acid; triethylamine; (-)-diisopinocamphenylborane chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride;
In
diethyl ether; dichloromethane; toluene; acetonitrile;
1.1: Aldol condensation / 1.2: Aldol condensation;
DOI:10.1039/c2ob25100k
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ozone / dichloromethane / -78 °C / Inert atmosphere
1.2: 4 h / -78 - 20 °C / Inert atmosphere
2.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere
2.2: 17 h / -78 - -20 °C / Inert atmosphere
3.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 21 h / -30 - -20 °C / Inert atmosphere
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / Molecular sieve; Inert atmosphere
5.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
6.1: dimethyl sulfide borane / toluene / 3 h / 100 °C / Inert atmosphere
With
2,6-dimethylpyridine; dimethyl sulfide borane; ozone; acetic acid; triethylamine; (-)-diisopinocamphenylborane chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride;
In
diethyl ether; dichloromethane; toluene; acetonitrile;
2.1: Aldol condensation / 2.2: Aldol condensation;
DOI:10.1039/c2ob25100k
