5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

Base Information

Chemical Name:5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide
CAS No.:960401-54-1
Molecular Formula:C₂₈H₃₆ClNO₃SSi
Molecular Weight:530.203
Hs Code.:

Synonyms:5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

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Chemical Property of 5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

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Technology Process of 5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

There total 4 articles about 5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 892870-41-6
3-methoxy-4-triisopropylsilanyloxy-phenylamine

: C₁₂H₈Cl₂OS

: 960401-54-1
5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.666667h;

Reference yield:

: 892870-40-5
triisopropyl-(2-methoxy-4-nitro-phenoxy)-silane

: 960401-54-1
5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 5%-palladium/activated carbon / ethanol / 8 h / 20 °C / 2585.81 Torr

2: triethylamine / dichloromethane / 0.67 h / 0 - 20 °C

With hydrogen; triethylamine; 5%-palladium/activated carbon; In ethanol; dichloromethane;

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 960401-54-1
5-(4-chloro-phenyl)-3-methyl-thiophene-2-carboxylic acid (3-methoxy-4-triisopropylsilanyloxy-phenyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 10 °C

1.2: 10 - 20 °C

2.1: hydrogen / 5%-palladium/activated carbon / ethanol / 8 h / 20 °C / 2585.81 Torr

3.1: triethylamine / dichloromethane / 0.67 h / 0 - 20 °C

With hydrogen; sodium hydride; triethylamine; 5%-palladium/activated carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;