dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

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Chemical Name:dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate
CAS No.:1242659-94-4
Molecular Formula:C₅₅H₇₄N₁₀O₁₇
Molecular Weight:1147.25
Hs Code.:

dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

Synonyms:dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

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Chemical Property of dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

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Technology Process of dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

There total 1 articles about dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2C₂HF₃O₂*C₂₄H₃₈N₂O₁₀

: sodium 3,5-bis-(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidino-methyl)benzoate

: 1242659-94-4
dimethyl 14-[2-[3,5-bis(1-(tert-butyloxycarbonyl)-3-(pyrrol-2-carbonyl)-guanidinomethyl)benzamido]-ethyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 - 40 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.06.024