tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

Base Information

Chemical Name:tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane
CAS No.:1154606-95-7
Molecular Formula:C₂₆H₃₄O₂Si
Molecular Weight:406.64
Hs Code.:

Synonyms:tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

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Chemical Property of tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

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Technology Process of tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

There total 1 articles about tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13944-75-7,24120-79-4,31750-20-6,33318-22-8,35644-74-7,35692-59-2,39903-74-7,39903-81-6,39903-82-7,128385-82-0
(1S,4S,6R)-4-Isopropenyl-1-methyl-7-oxa-bicyclo[4.1.0]heptan-2-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1154606-95-7
tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

Guidance literature:: With 1H-imidazole; In Triethylene glycol dimethyl ether; N,N-dimethyl-formamide; at 20 ℃; for 84h; Product distribution / selectivity;

Reference yield: 76.0%

: 1154606-95-7
tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane

: 1154606-96-8
(1R,3R,5R,6R)-5-{[tert-butyl(diphenyl)silyl]oxy}-6-methyl-7-oxabicyclo[4.1.0]heptan-3-ol

Guidance literature:: tert-butyl{[(1R,2R,4R,6R)-4-isopropenyl-1-methyl-7-oxabicyclo[4.1.0]hept-2-yl]oxy}diphenylsilane; With sodium hydrogencarbonate; ozone; In methanol; dichloromethane; water; ethyl acetate; at -70 ℃; under 362.013 - 413.729 Torr;

With pyridine; 4-nitro-benzoyl chloride; In dichloromethane; at 5 - 20 ℃;

With potassium carbonate; In methanol; water; for 2h;