(R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate

Base Information

• Chemical Name: (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate
• CAS No.: 1193310-78-9
• Molecular Formula: C₃₃H₅₄O₇Si
• Molecular Weight: 590.873

Synonyms:(R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate

Chemical Property of (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate

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Technology Process of (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate

There total 1 articles about (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsiloxy)propyl)tetrahydrofuran-2-yl)propanoic acid (1193310-77-8) + (R)-benzyl 2-((2R,5S)-5-((S)-2-hydroxypropyl)tetrahydrofuran-2-yl)propanoate (58106-10-8) → (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate (1193310-78-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 21 - 25 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ja9050235

Reference yield: 62.0%

(R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsilyloxy)propyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran-2-yl)propanoate (1193310-78-9) → (R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-hydroxypropyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran2-yl)propanoate (1193374-59-2)

Guidance literature:

With water; toluene-4-sulfonic acid; In acetic acid; at 21 - 25 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ja9050235

upstream raw materials:

(R)-2-((2R,5S)-5-((S)-2-(tert-butyldimethylsiloxy)propyl)tetrahydrofuran-2-yl)propanoic acid

(R)-benzyl 2-((2R,5S)-5-((S)-2-hydroxypropyl)tetrahydrofuran-2-yl)propanoate

Downstream raw materials:

(R)-benzyl 2-((2R,5S)-5-((S)-2-((R)-2-((2R,5S)-5-((S)-2-hydroxypropyl)tetrahydrofuran-2-yl)propanoyloxy)propyl)tetrahydrofuran2-yl)propanoate

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