di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate

Base Information

• Chemical Name: di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate
• CAS No.: 1211451-13-6
• Molecular Formula: C₃₀H₅₁N₅O₆
• Molecular Weight: 577.765

Synonyms:di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate

Chemical Property of di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate

Chemical Property:

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Technology Process of di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate

There total 1 articles about di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

di-tert-butyl (((5-nitroisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl))dicarbamate (1211451-12-5) → di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate (1211451-13-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; for 24h;

DOI:10.1002/chem.200902368

Reference yield:

di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate (1211451-13-6) + 2,2'-bipyridine-5-carbonyl chloride (140447-00-3) → di-tert-butyl (((5-([2,2'-bipyridine]-5-carboxamido)isophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl))dicarbamate (1262887-76-2)

Guidance literature:

With triethylamine; In chloroform; for 18h; Reflux; Inert atmosphere;

DOI:10.1039/c0cc04754f

Reference yield:

di-tert-butyl (((5-aminoisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl)) dicarbamate (1211451-13-6) + 2,2'-bipyridyl-4,4'-dicarboxylic acid chloride (72460-28-7) → tetra-tert-butyl (((5,5'-(([2,2'-bipyridine]-4,4'-dicarbonyl)bis(azanediyl))bis(isophthaloyl))tetrakis(azanediyl))tetrakis(hexane-6,1-diyl))tetracarbamate (1211451-14-7)

Guidance literature:

With triethylamine; In chloroform; at 0 - 20 ℃; Inert atmosphere; Reflux;

DOI:10.1002/chem.200902368

upstream raw materials:

di-tert-butyl (((5-nitroisophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl))dicarbamate

Downstream raw materials:

tetra-tert-butyl (((5,5'-(([2,2'-bipyridine]-4,4'-dicarbonyl)bis(azanediyl))bis(isophthaloyl))tetrakis(azanediyl))tetrakis(hexane-6,1-diyl))tetracarbamate

di-tert-butyl (((5-([2,2'-bipyridine]-5-carboxamido)isophthaloyl)bis(azanediyl))bis(hexane-6,1-diyl))dicarbamate

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