2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester

Base Information

• Chemical Name: 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester
• CAS No.: 102609-49-4
• Molecular Formula: C₂₆H₂₃N₃O₈
• Molecular Weight: 505.484

Synonyms:2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester

Chemical Property of 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester

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Technology Process of 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester

There total 2 articles about 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-nitrobenzyl 3-phenyl-2-aminopropionate (7413-82-3) + Chlorameisensaeure-N-5-hydroxy-norbornen-2,3-dicarboximidester (99502-89-3) → N-hydroxy-5-norbomene-2,3-dicarboxylic acid imide (1195164-50-1,397299-61-5) + 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester (102609-49-4)

Guidance literature:

With triethylamine; In dichloromethane; at -5 ℃; for 0.5h;

Reference yield:

4-nitrobenzyl 3-phenyl-2-aminopropionate (7413-82-3) + Chlorameisensaeure-N-5-hydroxy-norbornen-2,3-dicarboximidester (99502-89-3) → 2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester (102609-49-4)

Guidance literature:

With triethylamine; In dichloromethane;

Reference yield:

2-((1S,7R)-3,5-Dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yloxycarbonylamino)-3-phenyl-propionic acid 4-nitro-benzyl ester (102609-49-4) → 2-{3-[1-(4-Nitro-benzyloxycarbonyl)-2-phenyl-ethyl]-ureido}-3-phenyl-propionic acid 4-nitro-benzyl ester (114046-50-3)

Guidance literature:

With water; In 1,4-dioxane; at 80 - 90 ℃; for 0.333333h;

upstream raw materials:

4-nitrobenzyl 3-phenyl-2-aminopropionate

Chlorameisensaeure-N-5-hydroxy-norbornen-2,3-dicarboximidester

Downstream raw materials:

2-{3-[1-(4-Nitro-benzyloxycarbonyl)-2-phenyl-ethyl]-ureido}-3-phenyl-propionic acid 4-nitro-benzyl ester

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