N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester

Base Information

Chemical Name:N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester
CAS No.:1139906-45-8
Molecular Formula:C₅₂H₅₇N₃O₁₀
Molecular Weight:884.039
Hs Code.:

Synonyms:N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester

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Chemical Property of N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester

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Technology Process of N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester

There total 2 articles about N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129460-09-9,134098-70-7
Fmoc-Asp-O-t-Bu

: 522634-52-2
2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosylamine

: 1139906-45-8
N2-(9-fluorenylmethoxycarbonyl)-N4-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-aspargine tert-butyl ester

Guidance literature:: Fmoc-Asp-O-t-Bu; With 1-methyl-pyrrolidin-2-one; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h;

2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosylamine; In 1-methyl-pyrrolidin-2-one; dichloromethane; at 20 ℃;
DOI:10.1021/jm801577r