C₉H₈⁽²⁾HNO₂

Base Information

• Chemical Name: C₉H₈⁽²⁾HNO₂
• CAS No.: 1219743-54-0
• Molecular Formula: C₉H₉NO₂
• Molecular Weight: 164.168
• Mol file: 1219743-54-0.mol

Synonyms:C₉H₈⁽²⁾HNO₂

Chemical Property of C₉H₈⁽²⁾HNO₂

Chemical Property:

Purity/Quality:

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Technology Process of C₉H₈⁽²⁾HNO₂

There total 1 articles about C₉H₈⁽²⁾HNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

o-nitroiodobenzene (609-73-4) + C4H7(2)HO3S (307344-69-0) → C9H8(2)HNO2 (1219743-54-0)

Guidance literature:

o-nitroiodobenzene; With phenylmagnesium chloride; In tetrahydrofuran; at -40 ℃; Inert atmosphere;

With copper(l) cyanide; lithium chloride; In tetrahydrofuran; at -40 ℃; for 0.25h; Inert atmosphere;

C₄H₇⁽²⁾HO₃S; In tetrahydrofuran; at -40 ℃; Inert atmosphere;

DOI:10.1021/ol100220c

Reference yield:

C9H8(2)HNO2 (1219743-54-0) → 2-(2-deuterioallyl)aniline (1211481-32-1)

Guidance literature:

With acetic acid; zinc; Inert atmosphere;

DOI:10.1021/ol100220c

upstream raw materials:

o-nitroiodobenzene

C₄H₇⁽²⁾HO₃S

Downstream raw materials:

2-(2-deuterioallyl)aniline