methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:127529-69-5
Molecular Formula:C₅₈H₇₀N₂O₁₆
Molecular Weight:1051.2
Hs Code.:

methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Synonyms:methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 7 articles about methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127529-92-4
methyl 4-O-<3-O-(2-acetamido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 127529-69-5
methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With potassium carbonate; In 1,4-dioxane; methanol; at 0 ℃; for 16h;

Reference yield:

: 127529-67-3
4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 127529-69-5
methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / acetic acid / trifluoroacetic acid / 3 h / 0 - 20 °C

2: 84 percent / piperidine / tetrahydrofuran / 20 h

3: oxalyl bromide / dimethylformamide; CHCl₃ / 2 h / 0 - 20 °C

4: 95 percent / silver silicate aluminate, molecular sieves 3 Angstroem / toluene; CH₂Cl₂ / 1.5 h / -25 °C

5: NaSH / pyridine; H₂O / 23 h / Ambient temperature

6: pyridine / 0.5 h / Ambient temperature

7: 96 percent / K₂CO₃ / dioxane; methanol / 16 h / 0 °C

With piperidine; sodium hydrogensulfide; Oxalyl bromide; potassium carbonate; acetic acid; 3 A molecular sieve; silver silicate aluminate; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; trifluoroacetic acid;

Reference yield:

: 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α/β-D-glucopyranose

: 127529-69-5
methyl 4-O-<3-O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl bromide / dimethylformamide; CHCl₃ / 2 h / 0 - 20 °C

2: 95 percent / silver silicate aluminate, molecular sieves 3 Angstroem / toluene; CH₂Cl₂ / 1.5 h / -25 °C

3: NaSH / pyridine; H₂O / 23 h / Ambient temperature

4: pyridine / 0.5 h / Ambient temperature

5: 96 percent / K₂CO₃ / dioxane; methanol / 16 h / 0 °C

With sodium hydrogensulfide; Oxalyl bromide; potassium carbonate; 3 A molecular sieve; silver silicate aluminate; In 1,4-dioxane; pyridine; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene;