furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

Base Information

Chemical Name:furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone
CAS No.:1312713-59-9
Molecular Formula:C₂₀H₂₀F₃N₃O₃
Molecular Weight:407.392
Hs Code.:

Synonyms:furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

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Chemical Property of furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

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Technology Process of furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

There total 2 articles about furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1312713-69-1
furan-2-yl(2-isopropyl-4-methylenepyrazolidin-1-yl)methanone

: 74467-04-2
N-hydroxy-2-(trifluoromethyl)benzene-1-carbonimidoyl chloride

: 1312713-59-9
furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1021/jo200924y

Reference yield:

: 58431-00-8
N'-isopropylfuran-2-carbohydrazide

: 1312713-59-9
furan-2-yl(8-isopropyl-3-(2-(trifluoromethyl)phenyl)-1-oxa-2,7,8-triazaspiro[4.4]non-2-en-7-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice; Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/jo200924y