Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Base Information

Chemical Name:Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester
CAS No.:127762-04-3
Molecular Formula:C₁₈H₂₈BrNO₃
Molecular Weight:386.329
Hs Code.:

Synonyms:Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Suppliers and Price of Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

There total 4 articles about Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R,5R,8S)-1-((S)-4-Hydroxy-hept-6-enyl)-8-vinyl-6-oxa-bicyclo[3.2.1]octan-7-one

: 127762-04-3
Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / triphenylphosphine, carbon tetrabromide / diethyl ether / 2 h

2: AlMe₃, NH₄Cl / benzene / 40 h / 50 °C

3: pyridine, DMAP

With pyridine; dmap; carbon tetrabromide; trimethylaluminum; ammonium chloride; triphenylphosphine; In diethyl ether; benzene;
DOI:10.1021/ja00171a035

Reference yield:

: 127762-03-2
(1S,5R,8S)-1-((R)-4-Bromo-hept-6-enyl)-8-vinyl-6-oxa-bicyclo[3.2.1]octan-7-one

: 127762-04-3
Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AlMe₃, NH₄Cl / benzene / 40 h / 50 °C

2: pyridine, DMAP

With pyridine; dmap; trimethylaluminum; ammonium chloride; In benzene;
DOI:10.1021/ja00171a035

Reference yield:

: 127791-69-9
(1S,5R,8S)-1-[(S)-4-(tert-Butyl-dimethyl-silanyloxy)-hept-6-enyl]-8-vinyl-6-oxa-bicyclo[3.2.1]octan-7-one

: 127762-04-3
Acetic acid (1S,2S,3S)-3-((R)-4-bromo-hept-6-enyl)-3-carbamoyl-2-vinyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / 5percent HCl / tetrahydrofuran / 12 h

2: 61 percent / triphenylphosphine, carbon tetrabromide / diethyl ether / 2 h

3: AlMe₃, NH₄Cl / benzene / 40 h / 50 °C

4: pyridine, DMAP

With pyridine; hydrogenchloride; dmap; carbon tetrabromide; trimethylaluminum; ammonium chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/ja00171a035