C₂₅H₃₃NO₄S

Base Information

• Chemical Name: C₂₅H₃₃NO₄S
• CAS No.: 52719-99-0
• Molecular Formula: C₂₅H₃₃NO₄S
• Molecular Weight: 443.607
• Mol file: 52719-99-0.mol

Synonyms:C₂₅H₃₃NO₄S

Chemical Property of C₂₅H₃₃NO₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₃NO₄S

There total 8 articles about C₂₅H₃₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylbenzenesulfinyl chloride (10439-23-3) → C25H33NO4S (52719-99-0)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) Py, (ii) tBuOCl

2: aq. N₂H₄

3: Cl₂, Py

With pyridine; chlorine; hydrazine hydrate;

DOI:10.1021/ja00814a031

Reference yield:

(1R,2S,5R)-menthyl chloroformate (14602-86-9,7635-53-2) → C25H33NO4S (52719-99-0)

Guidance literature:

Multi-step reaction with 6 steps

1: NH₂OH*HCl, NaOAc

2: Et₃N

3: Et₃N / benzene

4: aq. N₂H₄

5: Cl₂, Py

With pyridine; hydroxylamine hydrochloride; sodium acetate; chlorine; hydrazine hydrate; triethylamine; In benzene;

DOI:10.1021/ja00814a031

Reference yield:

(-)-Menthyl-N-p-nitrobenzolsulfonoxycarbamat (52719-92-3) → C25H33NO4S (52719-99-0)

Guidance literature:

Multi-step reaction with 4 steps

1: Et₃N / benzene

2: aq. N₂H₄

3: Cl₂, Py

With pyridine; chlorine; hydrazine hydrate; triethylamine; In benzene;

DOI:10.1021/ja00814a031

upstream raw materials:

potassium p-methyl benzoate

(-)-(R)-N-[carbo-(1R)-menthoxy]-p-toluenesulfonimidoyl chloride

4-methylbenzenesulfinyl chloride

(1R,2S,5R)-menthyl chloroformate

Downstream raw materials:

C₁₉H₂₉NO₃S